Black Grape Juice Concentration via Ohmic-Vacuum Hybrid Heating: Quality Parameters, Energy Consumption and Exergy Efficiency

Document Type : Research Article

Authors

1 Department of Biosystems Engineering; Faculty of Agriculture; University of Kurdistan, Sanandaj, Kurdistan, Iran

2 Department of Horticultural Science, Faculty of Agriculture, University of Kurdistan, Sanandaj, Kurdistan, Iran

Abstract

In this study, the concentration process of black grape juice using a combined vacuum ohmic heating system was investigated, focusing on the effects of pressure parameters (50, 70, and 100 kPa) and voltage gradient (10, 20, and 30 V/cm) on processing time, specific energy consumption, exergy efficiency, and quality parameters (pH, total phenolic content, and antioxidant activity). The results indicated that increasing the voltage gradient significantly enhanced the heating rate and reduced processing time, while the combination of ohmic heating with vacuum (at 75 and 50 kPa) increased processing time. Specific energy consumption at atmospheric pressure (100 kPa) varied between 1.92 to 2.27 MJ/kg water, while reducing the pressure to 50 kPa led to an increase in specific energy consumption by 4.42 to 5.54 times. The highest exergy efficiency (18.78%) was observed at 100 kPa and a voltage gradient of 30 V/cm. In terms of quality, the reduction in pH (up to 16%) and the retention of total phenolic content (857 mg GAE/100 ml) and antioxidant activity (IC50 = 19.36%) at 50 kPa and a voltage gradient of 10 V/cm yielded the best quality results. Based on the findings, it can be suggested that optimizing the concentration process by selecting appropriate levels of pressure and voltage gradient to achieve a balance between energy efficiency and product quality could be explored in future studies.

Graphical Abstract

Black Grape Juice Concentration via Ohmic-Vacuum Hybrid Heating: Quality Parameters, Energy Consumption and Exergy Efficiency

Highlights

  • Higher voltages (20–30 V/cm) improved processing rate but reduced quality retention.
  • Lower pressures better preserved quality but increased energy demand.
  • The highest exergy efficiency (18.78%) was achieved at 30 V/cm and 100 kPa.
  • The best condition for quality retention was 10 V/cm and 50 kPa.

Keywords

Main Subjects


[1] Cosme, F., Pinto, T., & Vilela, A. (2018). Phenolic compounds and antioxidant activity in grape juices: A chemical and sensory view. Beverages, 4(1), 22. https://doi.org/10.3390/beverages4010022
[2] Tavares, H.M., Tessaro, I.C., & Cardozo, N.S.M. (2022). Concentration of grape juice: Combined forward osmosis/evaporation versus conventional evaporation. Innov. Food Sci. Emerg. Technol., 75, 102905. https://doi.org/10.1016/j.ifset.2021.102905
[3] Hosainpour, A., Darvishi, H., Nargesi, F., & Fadavi, A. (2014). Ohmic pre-drying of tomato paste. Food Sci. Technol. Int., (3), 193-204. https://doi.org/10.1177/1082013213480360
[4] Darvishi, H., Hosainpour, A., Nargesi, F., & Fadavi, A. (2015). Exergy and energy analyses of liquid food in an Ohmic heating process: A case study of tomato production. Innov. Food Sci. Emerg. Technol., 31, 73-82. https://doi.org/10.1016/j.ifset.2015.06.012
[5] Varghese, K. S., Pandey, M. C., Radhakrishna, K., & Bawa, A. (2014). Technology, applications and modelling of ohmic heating: A review. J. Food Sci. Technol., 51, 2304–2317. https://doi.org/10.1007/s13197-012-0710-3
[6] Yildiz, H., Icier, F., & Baysal, T. (2010). Changes in β-carotene, chlorophyll and color of spinach puree during ohmic heating. J. Food Process. Eng., 33, 763–779. https://doi.org/10.1111/j.1745-4530.2008.00303.x
[7] Kaur, N., & Singh, A.K. (2016). Ohmic heating: Concept and applications—a review. Crit. Rev. Food Sci. Nutr., 56(14), 2338–2351. https://doi.org/10.1080/10408398.2013.835303
[8] Fadavi, A., Yousefi, S., Darvishi, H., & Mirsaeedghazi, H. (2018). Comparative study of ohmic vacuum, ohmic, and conventional-vacuum heating methods on the quality of tomato concentrate. Innov. Food Sci. Emerg. Technol., 47, 225–230. https://doi.org/10.1016/j.ifset.2018.03.004
[9] Hwang, J.H., Jung, A.H., & Park, S.H. (2022). Efficacy of ohmic vacuum concentration for orange juice concentrates and their physicochemical properties under different voltage gradients. LWT, 154, 112750. https://doi.org/10.1016/j.lwt.2021.112750
[10] Darvishi, H., Mohammadi, P., Fadavi, A., Saba, M.K., & Behroozi-Khazaei, N. (2019). Quality preservation of orange concentrate by using hybrid ohmic–vacuum heating. Food Chem., 289, 292–298. https://doi.org/10.1016/j.foodchem.2019.03.043
[11] Alkanan, Z.T., Altemimi, A.B., Al-Hilphy, A.R., Cacciola, F., & Ibrahim, S.A. (2021). Application and effects of ohmic-vacuum combination heating on the quality factors of tomato paste. Foods, 10(12), 2920. https://doi.org/10.3390/foods10122920
[12] Sakr, M., & Liu, S. (2014). A comprehensive review on applications of ohmic heating (OH). Renew. Sustain. Energy Rev., 39, 262–269. https://doi.org/10.1016/j.rser.2014.07.061
[13] Cevik, M. (2021). Electrical conductivity and performance evaluation of verjuice concentration process using ohmic heating method. J. Food Process. Eng., 44(5), e13672. https://doi.org/10.1111/jfpe.13672
[14] Cokgezme, O.F., Sabanci, S., Cevik, M., Yildiz, H., & Icier, F. (2017). Performance analyses for evaporation of pomegranate juice in ohmic heating assisted vacuum system. J. Food Eng., 207, 1–9. https://doi.org/10.1016/j.jfoodeng.2017.03.015
[15] Darvishi, H., Behroozi-Khazaei, N., Koushesh Saba, M., Alimohammadi, Z., & Nourbakhsh, H. (2021). The influence of ohmic-vacuum heating on phenol, ascorbic acid and engineering factors of kiwifruit juice concentration process. Int. J. Food Sci. Technol., 56(9), 4789–4798. https://doi.org/10.1111/ijfs.15160
[16] Sabanci, S., & Icier, F. (2017). Applicability of ohmic heating assisted vacuum evaporation for concentration of sour cherry juice. J. Food Eng., 212, 262–270. https://doi.org/10.1016/j.jfoodeng.2017.06.004
[17] Bozkurt, H., & Icier, F. (2010). Exergetic performance analysis of ohmic cooking process. J. Food Eng., 100(4), 688–695. https://doi.org/10.1016/j.jfoodeng.2010.05.020
[18] Mohammadi, P., Amiri Chayjan, R., & Darvishi, H. (2025). Process production of date syrup using ohmic heating under vacuum: Evaluating the impact of voltage gradient and pressure on energy consumption, efficiency, and quality characteristics. Innov. Food Technol., 12(2), 192–211. https://doi.org/10.22104/ift.2025.7466.2204
[19] Sánchez-Moreno, C., Larrauri, J.A., & Saura-Calixto, F. (1999). A procedure to measure the antiradical efficiency of polyphenols. J. Sci. Food Agric., 76, 270–276. https://doi.org/10.1002/(SICI)1097-0010(199802)76:2<270::AID-JSFA945>3.0.CO;2-9
[20] Sabanci, S., & Icier, F. (2022). Evaluation of an ohmic assisted vacuum evaporation process for orange juice pulp. Food Bioprod. Process., 131, 156–163. https://doi.org/10.1016/j.fbp.2021.09.009
[21] Darvishi, H., Koushesh Saba, M., Behroozi-Khazaei, N., & Nourbakhsh, H. (2020). Improving quality and quantity attributes of grape juice concentrate (molasses) using ohmic heating. J. Food Sci. Technol., 57, 1362–1370. https://doi.org/10.1007/s13197-019-04170-1
[22] Hameed, A., Maan, A.A., Khan, M.K.I., Mahmood Khan, I., Niazi, S., Waheed Iqbal, M., Riaz, T., Manzoor, M.F., & Abdalla, M. (2023). Evaporation kinetics and quality attributes of grape juice concentrate as affected by microwave and vacuum processing. Int. J. Food Prop., 26(1), 1596–1611. https://doi.org/10.1080/10942912.2023.2218062
[23] Dinçer, C., Çam, İ.B., Torun, M., Gülmez, H.B., & Topuz, A. (2019). Mathematical modeling of concentrations of grape, pomegranate and black carrot juices by various methods. Gıda, 44(6), 1092–1105. https://doi.org/10.15237/gida.GD19080
[24] Sabanci, S., & Icier, F. (2020). Enhancement of the performance of sour cherry juice concentration process in vacuum evaporator by assisting ohmic heating source. Food Bioprod. Process., 122, 269–279. https://doi.org/10.1016/j.fbp.2020.05.004
[25] Samaranayake, P., & Sastry, S.K. (2005). Electrode and pH effects on electrochemical reactions during ohmic heating. J. Electroanal. Chem., 577, 125135. https://doi.org/10.1016/j.jelechem.2004.11.026
[26] Assiry, A.M., Gaily, M.H., Alsamee, M., & Sarifudin, A. (2010). Electrical conductivity of seawater during ohmic heating. Desalination, 260(1–3), 9–17. https://doi.org/10.1016/j.desal.2010.05.015
[27] Kaur, R., Gul, K., & Singh, A.K. (2016). Nutritional impact of ohmic heating on fruits and vegetables—A review. Cogent Food Agric., 2(1), 1159000. https://doi.org/10.1080/23311932.2016.1159000
[28] Pataro, G., Barca, G.M., Pereira, R.N., Vicente, A.A., Teixeira, J.A., & Ferrari, G. (2014). Quantification of metal release from stainless steel electrodes during conventional and pulsed ohmic heating. Innov. Food Sci. Emerg. Technol., 21, 66–73. https://doi.org/10.1016/j.ifset.2013.11.009
[29] Darvishi, H., Khoshtaghza, M.H., & Najafi, G. (2013). Ohmic heating of pomegranate juice: Electrical conductivity and pH change. J. Saudi Soc. Agric. Sci., 12, 101–108. https://doi.org/10.1016/j.jssas.2012.08.003
[30] Khairiyah, S., Sinaga, S.M., & De Putra, E. (2022). Determination of vitamin C and antioxidant activity in fresh red guava (Psidium guajava L.) and red guava commercial fruit juices. Int. J. Sci. Technol. Manag., 3(4), 880–883.  DOI: 10.46729/ijstm.v3i4.543
[31] Barrón-García, O.Y., Morales-Sánchez, E., Jiménez, A.R., Antunes-Ricardo, M., Luzardo-Ocampo, I., González-Jasso, E., & Gaytán-Martínez, M. (2022). Phenolic compounds profile and antioxidant capacity of ‘Ataulfo’ mango pulp processed by ohmic heating at moderate electric field strength. Food. Res. Int. 154, 111032. https://doi.org/10.1016/j.foodres.2022.111032
Volume 12, Issue 4
July 2025
Pages 321-337
  • Receive Date: 01 May 2025
  • Revise Date: 26 May 2025
  • Accept Date: 31 May 2025
  • First Publish Date: 31 May 2025
  • Publish Date: 31 May 2025